Asus A8N - SLI Deluxe
AMD Athlon 64 3200+
2GB DRAM Master [Micron Chips CL3 3-3-3-8] Memory PC3200 DDR400
160GB RAID0 Array [2x80GB Hitachi SATAII]
BFG 6800GT OC[Not OC By me....yet]
Alright, let me think here. If you memory is PC3200 and on a 333 divider with FSB at 250 then it should be running at 208 Mhz, which might be a problem since your memory seems to be generic brand. From my experiance on generic memory, they are typicly fairly poor oc'ers.
First you need to isolate the max speed of each of your main parts, CPU and Memory. To find your max memory speed, drop your CPU multiplier to something nuts like 7 (so when you hit a wall it can't possibly be your CPU) . Also Reduce your HTT multiplier to 3. Now, up the FSB in 3-5Mhz increments, each time running MemTest 86 for at least a pass or 2. This will take time, each memtest pass takes me about 40 min. Once you get errors start lowering the FSB in 1-2Mhz increments until you can get a few passes of Memtest with no errors.
Write down that speed.
Then increase your CPU multiplier back to its orignal number ( i think its 10 in your case). Put your ram on a 266 divider, or even something lower to take it out of the equation. Then up the FSB in the same 3-5Mhz increments. Each time boot to windows and run SuperPi on 32M digits, it should take 20-25min. If it fails, reduce the FSB by 1-2Mhz and try it again and again until you pass.
Write down that Speed.
Then you try and find a combination of FSB and RAM dividers that maxes out the speed of each. Keep as close to your CPU's max speed as possible, because that gives you the most boost in performance. If you search google there are sites that explain how to estimate RAM speed with dividers better than I, because it involves the ceiling function. Also adjust the HTT multiplier to keep the speed as close to 1000 as possible, there is 0 need to OC the HTT bus.
Adding voltage to the core once you hit an initial wall is dangerous, but not stupid. As the previous poster said, do it in the smallest increments possible. With air cooling I would strongly urge you to stay under 1.5v is possible. As for your RAM's voltage, since its generic, I am going to assume it like the standard DDR voltage range which is about 2.65v-2.9v. Anything above that is illadvised unless the RAM specificly states it will take it, or is warrantied.
Note all warranties will be voided,
If I missed something please feel free to correct me, or ask about it. This is a walkthrough off the top of my head from experiance on my board.