As a chemist, I have to say that pretty much ALL of the gases released in the entire process described are extremely hazardous to human health. Working beside a window isn't exactly ideal. A fumehood would have been much better, and please tell me you were wearing all the necessary equipment - gloves, safety glasses, labcoat, etc.
Now that all the Safety Trolling is over with - to speed things up (=D), the dissolving parts could have been done on a hot plate set to about 97 degrees Celsius, boiled down to a small fraction (extremely dangerous - hot acid + more fumes), and diluted back up again with deionized water. This would have reduced the process down to a mere couple of hours instead of waiting days for it to dissolve naturally.