Well, the good news is that those sticks are on the G.Skill memory configurator validation list for that motherboard. So compatibility isn't the issue for certain.
What BIOS version did you update to, out of curiosity? Your 9900k should have been supported since version 1005, so unless you were on a very old BIOS version, your BIOS version probably wasn't the reason the 9900k wasn't being recognized or working properly prior to updating. Probably the partial reset of the BIOS that happened because you updated, is why it began working.
Check for bent pins. Be aware that you are going to have to clean and repaste once you remove the CPU. The paste is not reusable after removal of the CPU cooler.
Once it's back together, if there are no bent pins, make sure you are ACTUALLY using slots 2 and 4. Often we see people thinking that 2 and four are counted from the edge of the motherboard in, but should actually be from the CPU socket moving outwards to the right. Note that ASUS has begun switching the locations of the A2 and B2 slots, from what all other board manufacturers are using. They are still the second and fourth slots, but unlike everybody else, ASUS is putting the A2 slot closest to the edge of the motherboard, rather than two slots over from the CPU.
If they ARE in the right slots, try removing the DIMM in the B2 slot, leaving only the DIMM installed in the A2 slot which is closest to the edge of the motherboard. Then do a hard reset of the BIOS. See if a single DIMM will run at the XMP profile properly. If it will, shut down, remove that DIMM and swap it out for the other one, restart and see if it still works properly with the second DIMM installed.
BIOS Hard Reset procedure
Power off the unit, switch the PSU off and unplug the PSU cord from either the wall or the power supply.
Remove the motherboard CMOS battery for five minutes. In some cases it may be necessary to remove the graphics card to access the CMOS battery.
During that five minutes, press the power button on the case, continuously, for 30 seconds. After the five minutes is up, reinstall the CMOS battery making sure to insert it with the correct side up just as it came out.
If you had to remove the graphics card you can now reinstall it, but remember to reconnect your power cables if there were any attached to it as well as your display cable.
Now, plug the power supply cable back in, switch the PSU back on and power up the system. It should display the POST screen and the options to enter CMOS/BIOS setup. Enter the bios setup program and reconfigure the boot settings for either the Windows boot manager or for legacy systems, the drive your OS is installed on if necessary.
Save settings and exit. If the system will POST and boot then you can move forward from there including going back into the bios and configuring any other custom settings you may need to configure such as Memory XMP, A-XMP or D.O.C.P profile settings, custom fan profile settings or other specific settings you may have previously had configured that were wiped out by resetting the CMOS.
In some cases it may be necessary when you go into the BIOS after a reset, to load the Optimal default or Default values and then save settings, to actually get the hardware tables to reset in the boot manager.