Is your main HDD on the older PATA standard?
Those VIA chipsets have a horrible tendency to 'lose' the SATA controller over a certain FSB setting. Your best bet would be to install a separate SATA controller card and use that, or (for preference) go for a board with more overclock-friendly core logic.
The alternative is to see if the board will go for the BSel mod. If it will, then you can strap that chip from a 200MHz FSB to, say, 266MHz.
Apparently what causes this is all of the system buses in a VIA chipset are permanently locked in ratio, so if you take the FSB too high then it raises the PCI bus, taking the SATA controller out of specification and 'losing' it.