Welcome to the forums my friend!
Unfortunately mixed modules are only guaranteed in the form sold (from the same pack). It's a 50/50 gamble whether mixed modules work, regardless as to whether they the same make/model/timings. This is due to how the manufacturing process changes over time.
So 2 modules of the exact same model but from 2 different packs could not be compatible. Only way to find out is to try. Not saying it never works, just it's 50/50. It's best practice to buy a whole new pack to avoid any potential headache.
Have you tried the new RAM module just by itself?
What is the rest of your system spec?
Have you reset CMOS?